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New Gold Analysis Instrument For Assay Lab

Topics [ gold bullion gold refinery silver ]

REFINERY

Michael Koch, Analytical Services Manager, reports that The Perth Mint Refinery is investing in sophisticated new instrumentation for analysing the purity of precious metals.

The Refinery is eagerly awaiting the arrival and commissioning of a Panalytical wavelength dispersive X-Ray Fluorescence (XRF) instrument. Due for delivery in June, and at a cost of $470,000, this represents a significant investment in new technology for the Assay laboratory. 

The instrument was purchased initially to supplement the analysis of fine gold bar samples, but will be expanded to include silver in mines, dore and other sample types once suitable methods are developed. The technique measures the fluorescent emissions produced when a sample is irradiated by an x-ray source to determine its elemental composition.

Currently, fine gold analysis is carried out by gravimetric fire assay which has been used for well over 100 years, but is still the recognised method of analysis by the industry.

For this reason, the XRF will not replace fire assay, but will be used in conjunction with the technique to reduce analysis times. It is estimated that the XRF will reduce fire assay analysis of fine gold bar samples by 75%.

The initial commissioning of the instrument for fine gold analysis is expected to be completed within three months of delivery.

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2 Comments

  • April 05 2012

    goldpelican says:

    What sort of depth can this penetrate for analysis? Many of the "low end" commercial XRF devices in the $20,000 range can only do 20-40 microns, would be interesting to see what a machine of this type can do. Full penetration through a kilo gold bar?
  • April 05 2012

    Michael Koch says:

    Hi Goldpelican

    It’s difficult to quote a definitive figure as there are a number of variables that will determine the critical depth that the X-rays penetrate the surface. This includes the sample density, composition and absorption of the primary and secondary X-rays produced . The new instrument utilises a 4.2KW primary X-ray source which is significantly better that the entry level units, however it’s primary purpose is to increase the intensity of secondary fluorescent X-rays to measure its elemental composition. So it’s more a function of  increasing our ability to measure impurities at a lower levels rather than to penetrate the sample to a greater depth. I hope this answers your question.

    Regards

    Michael Koch
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